Wednesday, 2 August 2017

TEXTILE CHEMICAL

HOW TO FIND PERCENTAGE PURITY OF ACETIC ACID


   Chemical formula                         CH3COOH
   Molecular weight                          60 gm/mole
   Equivalent weight                         60 gm/mole
   Form                                             Liquid
   Smell                                            Pungent
   Solubility                                      Good


    Acetic acid is a volatile organic acid. it is used in wet processing i.e. bleaching, dyeing and printing and finishing to maintain the pH on the acidic side i.e. - 7.

  Method to find our percentage purity :

    About 1 -2 gm of acetic acid is dissolved in 250 ml of distilled water in a measuring flask and 10 ml of this solution is tit rated against 0.1 N standard NaoH solution using phenolphthalein as an indicator. In this method end point is colorless to pink.

   Chemical  Reaction :

    CH3COOH         +     NaoH    ------------------------------>  CH3COONa     +  H2O
   Acetic acid             Sodium           Neutralization        Sodium acetate     water 
                               Hydroxide 


    Formula :

   Percentage     E.Q of CH3COOH x N. of NaOH x B.R           250    
   purity of    =  ------------------------------------------------- x   -----   x 100
   acetic acid      1000 x weight of  acetic acid dissolved in    10
                                                         250 ml

            E.Q = Equivalent weight
            N     = Normality
            B.R = Burette reading
                                                 
                                                                  -------------% 

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